Structures by: Reisner E.
Total: 78
C108H253Br7Co6O75Ti27
C108H253Br7Co6O75Ti27
Chemical Science (2012) 3, 8 2470
a=23.8831(4)Å b=20.6857(3)Å c=20.2699(3)Å
α=90.00° β=92.5460(10)° γ=90.00°
[CoCl(dmgH)2(C5H4N-PO3Et2)]
C17H28ClCoN5O7P
Faraday Discussions (2012) 155, 191
a=8.2787(6)Å b=12.8802(10)Å c=21.4315(18)Å
α=90.00° β=94.937(7)° γ=90.00°
Trans-[Dichlorotetraindazoleruthenium(III)]chloride methanol disolvate
C30H32Cl3N8O2Ru
Journal of medicinal chemistry (2005) 48, 8 2831-2837
a=17.681(4)Å b=11.082(2)Å c=16.738(3)Å
α=90.00° β=102.46(3)° γ=90.00°
Trans-[Dichlorotetraindazoleruthenium(II)]acetone disolvate
C34H36Cl2N8O2Ru
Journal of medicinal chemistry (2005) 48, 8 2831-2837
a=10.891(2)Å b=13.279(3)Å c=14.399(3)Å
α=65.66(3)° β=69.04(3)° γ=68.36(3)°
Cis,cis,cis- dichlorobis(dimethylsulfoxide)bis(indazole)ruthenium(ii)
C18H24Cl2N4O2RuS2
Dalton transactions (Cambridge, England : 2003) (2005) 14 2355-2364
a=12.194(2)Å b=12.888(3)Å c=14.720(3)Å
α=90.00° β=107.68(3)° γ=90.00°
Trans,cis,cis- dichlorobis(dimethylsulfoxide)bis(indazole)ruthenium(ii)
C18H24Cl2N4O2RuS2
Dalton transactions (Cambridge, England : 2003) (2005) 14 2355-2364
a=11.833(2)Å b=13.477(3)Å c=16.340(3)Å
α=113.96(3)° β=97.57(3)° γ=104.00(3)°
Trans,trans,trans- dichlorobis(dimethylsulfoxide)bis(indazole)ruthenium(ii)
C22H36Cl2N4O4RuS4
Dalton transactions (Cambridge, England : 2003) (2005) 14 2355-2364
a=27.0678(5)Å b=7.8991(5)Å c=14.0096(3)Å
α=90.00° β=94.1198(12)° γ=90.00°
Trans-dichlorobis(dimethylsulfoxide)amidineruthenium(ii) monohydrate
C13H23Cl2N3O3RuS2
Dalton transactions (Cambridge, England : 2003) (2005) 14 2355-2364
a=17.726(4)Å b=8.367(2)Å c=14.415(3)Å
α=90.00° β=113.56(3)° γ=90.00°
Trans- dichloro(dimethylsulfoxide)(indazole)amidineruthenium(ii) acetonitrile
C20H24Cl2N6ORuS
Dalton transactions (Cambridge, England : 2003) (2005) 14 2355-2364
a=12.235(2)Å b=14.800(3)Å c=13.614(3)Å
α=90.00° β=105.69(3)° γ=90.00°
C93H63Cu2N11O2P4
C93H63Cu2N11O2P4
Dalton Transactions (2012) 41, 19 5919
a=11.0066(2)Å b=12.5966(2)Å c=16.6026(3)Å
α=98.7170(10)° β=100.8340(10)° γ=113.5480(10)°
C36H30AuP21,C10N51
C36H30AuP21,C10N51
Dalton Transactions (2012) 41, 19 5919
a=11.3138(2)Å b=12.4831(2)Å c=15.4936(4)Å
α=69.145(1)° β=81.391(1)° γ=69.918(1)°
C92H60Ag2N10P4,CHCl3
C92H60Ag2N10P4,CHCl3
Dalton Transactions (2012) 41, 19 5919
a=10.9813(1)Å b=12.7250(2)Å c=16.8652(3)Å
α=97.866(1)° β=100.456(1)° γ=112.374(1)°
C100.5H78Cu2N10P6
C100.5H78Cu2N10P6
Dalton Transactions (2012) 41, 19 5919
a=12.7176(2)Å b=14.3620(2)Å c=15.2562(2)Å
α=114.1120(10)° β=101.5560(10)° γ=106.3640(10)°
C21H19NiS3Se1,C16H36N1
C21H19NiS3Se1,C16H36N1
Dalton transactions (Cambridge, England : 2003) (2014) 43, 11 4483-4493
a=18.6006(4)Å b=23.1712(5)Å c=18.7401(5)Å
α=90.00° β=109.268(1)° γ=90.00°
C21H19Ni1S41,C16H36N11
C21H19Ni1S41,C16H36N11
Dalton transactions (Cambridge, England : 2003) (2014) 43, 11 4483-4493
a=18.5275(2)Å b=23.1544(2)Å c=18.7038(2)Å
α=90.00° β=109.270(1)° γ=90.00°
C21H19NiS3Se1,C16H36N1
C21H19NiS3Se1,C16H36N1
Dalton transactions (Cambridge, England : 2003) (2014) 43, 11 4483-4493
a=18.7224(2)Å b=23.0398(2)Å c=18.7818(2)Å
α=90.00° β=109.810(1)° γ=90.00°
C21H19NiS2Se21,C16H36N1
C21H19NiS2Se21,C16H36N1
Dalton transactions (Cambridge, England : 2003) (2014) 43, 11 4483-4493
a=10.6327(2)Å b=22.5152(5)Å c=16.1237(5)Å
α=90.00° β=94.708(1)° γ=90.00°
(NEt3H)[CoCl(dmgH)2(C5H4N-PO3H)]*0.5MeOH
C19H35ClCoN6O7P,C0.5H2O0.5
Chem.Commun. (2011) 47, 1695
a=8.171(5)Å b=12.998(5)Å c=14.602(5)Å
α=113.768(5)° β=99.000(5)° γ=97.294(5)°
C51H119CoIO31Ti11,(C3H8O)0.5
C51H119CoIO31Ti11,(C3H8O)0.5
Chem. Commun. (2013) 49, 4331
a=14.917(6)Å b=13.821(5)Å c=20.851(8)Å
α=90.00° β=90.191(7)° γ=90.00°
C51H119CoIO31Ti11,(C3H8O)0.5
C51H119CoIO31Ti11,(C3H8O)0.5
Chem. Commun. (2013) 49, 4331
a=14.917(6)Å b=13.821(5)Å c=20.851(8)Å
α=90.00° β=90.191(7)° γ=90.00°
2(C14H21ClCoN5O5),C4H10O
2(C14H21ClCoN5O5),C4H10O
Physical chemistry chemical physics : PCCP (2014) 16, 12 5739-5746
a=8.0000(1)Å b=13.5322(2)Å c=19.2803(3)Å
α=90.00° β=92.183(1)° γ=90.00°
Et4N[Fe(S-p-tolyl)2(NO)2]
C22H34FeN3O2S2,C2H4O0.5
Journal of the American Chemical Society (2008) 130, 15602-15610
a=8.979(3)Å b=30.661(10)Å c=10.361(3)Å
α=90.00° β=103.129(5)° γ=90.00°
Acetylpyrazine ^4^N-phenylthiosemicarbazone
C13H13N5S
Inorganic Chemistry (2008) 47, 11032-11047
a=5.7844(14)Å b=10.036(3)Å c=11.314(4)Å
α=76.005(12)° β=87.021(9)° γ=89.220(9)°
N,N-dimethyl-2-(1-pyridin-2-ylethyl)hydrazinecarbothioamide
C10H16N4S
Inorganic Chemistry (2008) 47, 11032-11047
a=5.4716(2)Å b=18.9799(7)Å c=11.8689(4)Å
α=90.00° β=97.289(2)° γ=90.00°
[Bis(acetylpyrazine ^4^N-phenylthiosemicarbazonato)-N,N,S-gallium(III)] nitrate monohydrate
C26H26GaN11O4S2
Inorganic Chemistry (2008) 47, 11032-11047
a=14.9818(5)Å b=22.0746(7)Å c=8.6006(3)Å
α=90.00° β=90.00° γ=90.00°
Mer-trichlorotripyrazoloruthenium(III)
C9H12Cl3N6Ru
Inorganic Chemistry (2005) 44, 6704-6716
a=18.936(4)Å b=8.028(2)Å c=19.180(4)Å
α=90.00° β=91.64(3)° γ=90.00°
Mer-trichlorotripyrazoloruthenium(III)
C33H38Cl3N8O2Ru
Inorganic Chemistry (2005) 44, 6704-6716
a=15.748(3)Å b=13.699(3)Å c=16.564(3)Å
α=90.00° β=93.66(3)° γ=90.00°
Mer-trichlorotripyrazoloruthenium(III)
C12H18Cl3N6Ru
Inorganic Chemistry (2005) 44, 6704-6716
a=11.313(2)Å b=11.546(2)Å c=13.456(3)Å
α=90.00° β=90.00° γ=90.00°
Mer-trichlorotripyrazoloruthenium(III)
C12H16Cl3N8Ru
Inorganic Chemistry (2005) 44, 6704-6716
a=9.6322(19)Å b=18.979(4)Å c=9.6991(19)Å
α=90.00° β=90.01(3)° γ=90.00°
Mer-trichlorotripyrazoloruthenium(III)
C12H16Cl3N8Ru
Inorganic Chemistry (2005) 44, 6704-6716
a=7.9169(16)Å b=8.4136(17)Å c=14.658(3)Å
α=102.90(3)° β=90.93(3)° γ=110.60(3)°
Mer-trichlorotripyrazoloruthenium(III)
C8H16Cl2F6N12O2RuSb
Inorganic Chemistry (2005) 44, 6704-6716
a=7.4500(15)Å b=7.6149(15)Å c=10.550(2)Å
α=81.82(3)° β=88.66(3)° γ=63.26(3)°
Mer-trichlorotripyrazoloruthenium(III)
C9H15Cl3N9Ru
Inorganic Chemistry (2005) 44, 6704-6716
a=7.1390(10)Å b=19.878(4)Å c=12.167(2)Å
α=90.00° β=92.62(3)° γ=90.00°
Mer-trichlorotripyrazoloruthenium(III)
C18H30B2F8N18Ru
Inorganic Chemistry (2005) 44, 6704-6716
a=12.194(2)Å b=12.194(2)Å c=17.336(3)Å
α=90.00° β=90.00° γ=120.00°
Mer-trichlorotripyrazoloruthenium(III)
C21H36Cl3N6Ru
Inorganic Chemistry (2005) 44, 6704-6716
a=17.730(4)Å b=10.794(2)Å c=27.802(6)Å
α=90.00° β=90.35(3)° γ=90.00°
Trans,trans,trans-[Diichlorobis(indazole)bis(dimethyl sulphide) ruthenium(II)]
C18H24Cl2N4RuS2
Inorganic Chemistry (2005) 44, 122-132
a=15.725(3)Å b=9.883(2)Å c=14.080(3)Å
α=90.00° β=102.39(3)° γ=90.00°
Mer-[Trichlorobis(indazole)(dimethyl sulphide)ruthenium(III)]
C18H22Cl3N4RuS
Inorganic Chemistry (2005) 44, 122-132
a=17.029(3)Å b=12.393(2)Å c=20.013(4)Å
α=90.00° β=90.91(3)° γ=90.00°
Mer-[Trichlorobis(indazole)(9-methyladenine)ruthenium(III)].CH2Cl2.CH3OH
C22H25Cl5N9ORu
Inorganic Chemistry (2005) 44, 122-132
a=9.486(2)Å b=11.427(2)Å c=13.972(3)Å
α=102.31(3)° β=98.72(3)° γ=98.82(3)°
Mer-[Trichlorobis(indazole)(9-methyladenine)ruthenium(III)].1.1H2O .0.9CH3OH
C21H24.5Cl3N9O2Ru
Inorganic Chemistry (2005) 44, 122-132
a=14.834(3)Å b=9.763(2)Å c=18.102(4)Å
α=90.00° β=100.33(3)° γ=90.00°
Mer,trans-[Trichloridoindazole-1-(1H-indazol-1-yl)ethanimineruthenium(III) diethyl ether solvate
C20H25Cl3N5ORu
Inorganic Chemistry (2008) 47, 6513-6523
a=21.2476(8)Å b=13.0596(8)Å c=16.8248(6)Å
α=90.00° β=96.347(4)° γ=90.00°
Mer,trans-[Trichloridobis(indazole)(kappa^N3^-N6,N6- dimethyladenineruthenium(III)] tetrahydrofuran solvate
C25H29Cl3N9ORu
Inorganic Chemistry (2008) 47, 6513-6523
a=10.690(2)Å b=12.757(3)Å c=12.957(3)Å
α=116.63(3)° β=103.45(3)° γ=103.08(3)°
Mer,trans-[Trichloridoindazole-1-(1H-indazol-1-yl-1- phenylmethanimineruthenium(III)] benzonitrile solvate
C28H22Cl3N6Ru
Inorganic Chemistry (2008) 47, 6513-6523
a=9.808(2)Å b=11.927(2)Å c=12.689(3)Å
α=104.96(3)° β=107.96(3)° γ=93.78(3)°
Trans,trans-[Dichlorido-bis(1-(1H-indazol-1-yl)ethanimine)ruthenium(III)] acetonitrile solvate
C20H21Cl3N7Ru
Inorganic Chemistry (2008) 47, 6513-6523
a=9.1416(8)Å b=10.5096(7)Å c=13.0426(12)Å
α=102.157(6)° β=106.752(7)° γ=95.512(6)°
Mer,trans-[Trichloridobis(indazole)methanolruthenium(III)]
C16H20Cl3N4O2Ru
Inorganic Chemistry (2008) 47, 6513-6523
a=8.1718(3)Å b=12.0086(5)Å c=21.2128(8)Å
α=90.00° β=99.626(3)° γ=90.00°
Sodium trans-[tetrachloridobis(indazole)ruthenate(III)] ethyl acetate adduct
C22H28Cl4N4NaO4Ru
Inorganic Chemistry (2008) 47, 6513-6523
a=6.5950(4)Å b=7.7044(4)Å c=14.1038(8)Å
α=75.446(3)° β=83.563(4)° γ=84.134(3)°
Mer,trans-[Monoaquatrichloridobis(indazole)ruthenium(III)]
C14H14Cl3N4ORu
Inorganic Chemistry (2008) 47, 6513-6523
a=23.2227(13)Å b=24.8073(13)Å c=8.6427(5)Å
α=90.00° β=94.679(6)° γ=90.00°
Indazolium trans-tetrachlorodimethylsulfoxide(indazole)ruthenate(III)
C16H19Cl4N4ORuS
Inorganic Chemistry (2004) 43, 7083-7093
a=10.619(2)Å b=8.691(2)Å c=22.667(5)Å
α=90.00° β=103.00(3)° γ=90.00°
Benzyltriphenylphosphonium trans-tetrachlorodimethyl- sulfoxidetriazoleruthenate(III)
C29H31Cl4N3OPRuS
Inorganic Chemistry (2004) 43, 7083-7093
a=9.599(2)Å b=12.680(3)Å c=14.476(3)Å
α=112.15(3)° β=109.16(3)° γ=90.90(3)°
Bis(triphenylphosphoranylidene)ammonium trans-tetrachloro- dimethylsulfoxidetriazoleruthenate(III)
C40H39Cl4N4OP2RuS
Inorganic Chemistry (2004) 43, 7083-7093
a=17.029(3)Å b=16.428(3)Å c=14.653(3)Å
α=90.00° β=103.32(3)° γ=90.00°
Indazolindazolium trans-tetrachloro(indazole)ruthenate(III)
C14H12.5Cl2N4Ru0.5
Inorganic Chemistry (2004) 43, 7083-7093
a=6.6020(10)Å b=9.962(2)Å c=11.671(2)Å
α=92.78(3)° β=102.57(3)° γ=104.75(3)°
Triazolium cis-tetrachloro-bis(triazole)ruthenate(III)
C6H12Cl4N9ORu
Inorganic Chemistry (2003) 42, 6024-6031
a=9.474(2)Å b=8.794(2)Å c=18.343(4)Å
α=90.00° β=94.40(3)° γ=90.00°
Triphenylbenzylphosphonium trans-tetrachloro-bis(triazole)ruthenate(III)
C29H30Cl4N6OPRu
Inorganic Chemistry (2003) 42, 6024-6031
a=11.605(2)Å b=17.149(3)Å c=16.023(3)Å
α=90.00° β=97.81(3)° γ=90.00°
[Fe4(O2Cbiph)8(THF)2]
C112H88Fe4O18
Inorganic chemistry (2007) 46, 25 10754-10770
a=13.1530(19)Å b=25.159(4)Å c=14.097(2)Å
α=90.00° β=93.854(3)° γ=90.00°
[Fe4(O2Cbiph)8(Hind)2]
C118H84Fe4N4O16,2(CH2Cl2)
Inorganic chemistry (2007) 46, 25 10754-10770
a=14.0208(15)Å b=14.2725(15)Å c=15.7331(16)Å
α=109.966(2)° β=96.596(2)° γ=115.812(2)°
[Fe4(O2Cbiph)8(pyrazole)2]
C110H80Fe4N4O16
Inorganic chemistry (2007) 46, 25 10754-10770
a=13.559(6)Å b=24.633(11)Å c=13.817(6)Å
α=90.00° β=96.444(9)° γ=90.00°
[Fe4(dimepz)2]4CH2Cl2
C114H88Fe4N4O16,4(CH2Cl2)
Inorganic chemistry (2007) 46, 25 10754-10770
a=13.2698(7)Å b=13.7009(7)Å c=29.8852(16)Å
α=93.2150(10)° β=94.7490(10)° γ=91.0210(10)°
[Fe4(O2Cbiph)8(acetamide)2]2C6H5Cl
C108H82Fe4N2O18,2(C6H5Cl)
Inorganic chemistry (2007) 46, 25 10754-10770
a=13.955(3)Å b=14.181(3)Å c=15.806(3)Å
α=109.421(3)° β=95.956(3)° γ=116.237(3)°
[Fe3(O2Cbiph)6(MeCN)4]
C86H66Fe3O12
Inorganic chemistry (2007) 46, 25 10754-10770
a=12.598(2)Å b=12.617(2)Å c=13.368(2)Å
α=71.827(3)° β=83.311(3)° γ=64.997(3)°
[Fe3(O2Cbiph)6(MeCN)4]CH2Cl2
C86H66Fe3N4O12,CH2Cl2
Inorganic chemistry (2007) 46, 25 10754-10770
a=13.496(2)Å b=13.766(3)Å c=23.334(4)Å
α=92.783(3)° β=102.073(3)° γ=117.536(3)°
[Fe3(O2Cbiph)6(dme)2]
C86H74Fe3O16
Inorganic chemistry (2007) 46, 25 10754-10770
a=12.222(13)Å b=12.345(9)Å c=13.650(11)Å
α=104.55(2)° β=115.45(2)° γ=90.96(3)°
[Fe2(O2Cbiph)4(py)2]CH2Cl2
C62H46Fe2N2O8,CH2Cl2
Inorganic chemistry (2007) 46, 25 10754-10770
a=24.960(7)Å b=10.012(3)Å c=21.217(6)Å
α=90.00° β=92.282(5)° γ=90.00°
[Fe2(O2Cbiph)4(1-meim)2]CH2Cl2
C60H48Fe2N4O8,CH2Cl2
Inorganic chemistry (2007) 46, 25 10754-10770
a=24.769(10)Å b=10.586(6)Å c=20.607(10)Å
α=90.00° β=91.00(4)° γ=90.00°
[Fe2(Tol)2(Ph,Xyl)2(THF)2]2CH2Cl2
C92H84O10Fe2,C2H4Cl4
Inorganic chemistry (2007) 46, 24 10229-10240
a=12.2604(12)Å b=17.6170(17)Å c=20.0356(19)Å
α=90.00° β=92.308(2)° γ=90.00°
[Fe2(Ph,Xyl)4(THF)2]1/2CH2Cl2
C92H84Fe2O10,C0.5HCl
Inorganic chemistry (2007) 46, 24 10229-10240
a=12.9614(19)Å b=23.089(3)Å c=13.1367(19)Å
α=90.00° β=99.373(2)° γ=90.00°
[Fe2(m-Tol)2(Ph,Xyl)2(py)2]4CH2Cl2
C94H78Fe2N2O8,4(CH2Cl2)
Inorganic chemistry (2007) 46, 24 10229-10240
a=12.313(4)Å b=17.466(6)Å c=20.457(7)Å
α=90.00° β=93.745(5)° γ=90.00°
[Fe2(Ph,Xyl)4(py)2]
C94H78Fe2N2O8
Inorganic chemistry (2007) 46, 24 10229-10240
a=11.707(3)Å b=14.289(4)Å c=24.133(6)Å
α=93.286(5)° β=95.981(5)° γ=111.166(4)°
[Fe2(O2CArTol)4(MeSCH2py)]CH2Cl2Et2O
C91H77Fe2NO8S,C4H10O,CH2Cl2
Inorganic chemistry (2007) 46, 24 10229-10240
a=12.9047(7)Å b=27.1966(15)Å c=23.0779(13)Å
α=90.00° β=92.6130(10)° γ=90.00°
[Fe2(O2CArTol)4(pyCH2SEt)]
C92H79Fe2NO8S,2(CH2Cl2)
Inorganic chemistry (2007) 46, 24 10229-10240
a=12.9053(10)Å b=26.771(2)Å c=23.6564(19)Å
α=90.00° β=94.1390(10)° γ=90.00°
[Fe2(O2CArTol)4(tBuSCH2py)]C6H5Cl1/4pentane
C94H83Fe2NO8S,C6H5Cl,0.25(C5H12)
Inorganic chemistry (2007) 46, 24 10229-10240
a=25.1545(18)Å b=25.3801(17)Å c=13.7159(9)Å
α=90.00° β=90.00° γ=90.00°
[Fe2(O2CArTol)4(MesPhSCH2py)]
C99H85Fe2NO8S,(C6H5Cl)
Inorganic chemistry (2007) 46, 24 10229-10240
a=24.7949(18)Å b=26.2886(19)Å c=13.7704(10)Å
α=90.00° β=90.00° γ=90.00°
[Fe2(O2CArXyl,Ph)4(pyCH2SMes)]
C99H85Fe2NO8S,C7.25H8Cl
Inorganic chemistry (2007) 46, 24 10229-10240
a=19.538(19)Å b=14.946(15)Å c=35.12(3)Å
α=90.00° β=105.542(18)° γ=90.00°
[FeCl2(meim)4]
C16H24Cl2Fe1N8
Inorganic chemistry (2007) 46, 25 10754-10770
a=7.5094(9)Å b=16.123(2)Å c=8.9317(11)Å
α=90.00° β=107.308(2)° γ=90.00°
[Fe2(O2CArTol)4(pyCH2SPh)]
C96H79Fe2NO8S,C4.5H5.5Cl3.5
Inorganic chemistry (2007) 46, 24 10229-10240
a=16.5043(10)Å b=26.2368(15)Å c=21.0392(12)Å
α=90.00° β=96.0190(10)° γ=90.00°
[Fe2(O2CArTol)4(pyCH2OEt)
C92H81Fe2NO9,CH2Cl2,C3H7.5O0.75
Inorganic chemistry (2007) 46, 24 10229-10240
a=12.9375(11)Å b=26.992(2)Å c=23.441(2)Å
α=90.00° β=93.893(2)° γ=90.00°
[Fe2(O2CArTol)4(iPr3PhSCH2py)]
C107H97Fe2NO8S,C12.5H16Cl2
Inorganic chemistry (2007) 46, 24 10229-10240
a=12.8583(8)Å b=15.4052(10)Å c=27.3385(18)Å
α=88.8720(10)° β=78.0520(10)° γ=71.6660(10)°
C64H45AgN5P3
C64H45AgN5P3
Dalton Transactions (2012) 41, 19 5919
a=12.6870(1)Å b=25.7466(2)Å c=16.6696(2)Å
α=90.00° β=93.4460(10)° γ=90.00°
Mer-trichlorotripyrazoloruthenium(III)
C6H11Cl3N9ORu
Inorganic Chemistry (2005) 44, 6704-6716
a=8.1046(16)Å b=14.693(3)Å c=11.754(2)Å
α=90.00° β=98.29(3)° γ=90.00°
[Fe4(O2Cbiph)4(Hdimepz)2]2CH2Cl2
C114H88Fe4N4O16,2(CH2Cl2)
Inorganic chemistry (2007) 46, 25 10754-10770
a=13.2541(17)Å b=14.0636(19)Å c=16.056(2)Å
α=97.388(2)° β=101.633(2)° γ=116.504(2)°
[Fe3(O2Cbiph)6(THF)4]
C94H86Fe3O16
Inorganic chemistry (2007) 46, 25 10754-10770
a=13.776(2)Å b=14.849(2)Å c=22.949(5)Å
α=94.328(4)° β=105.652(3)° γ=117.224(2)°